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This study aims to determine the quality of physics objective test High Order Thinking (HOT) in the temperature and heat material that fulfills good qualifications which include aspects of validity, reliability, level of difficulty, differentiating power and effectiveness of deceivers used in the learning assessment process as learning evaluation materials. This research includes research development (research and development) with the Borg and Gall model. Distribution of material in research on expansion, heat relationship with object temperature and shape, the principle of Black, heat transfer, ideal gas and thermodynamics. From each question material, several competency questions are obtained as a reference in making questions. This HOT test can be used as a standard test to measure students high-level abilities on high temperature and heat material in high school.