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This study aims to determine the basic technique of teaching materials in the analysis of the basic analytical chemistry courses that have met the feasibility of BSNP. This research includes research and development with the model of development of the Analysis-Design-Development-Implementation-Evaluation (ADDIE) model. The sample was selected using a purposive sampling technique. The sample in this study were two student handbooks which are commonly used in the Basic Analytical Chemistry course at FMIPA UNIMED and two classes in the Department of Chemistry FMIPA UNIMED as many as 40 students. Data of the research results are then analyzed by using SPPS 21.0 for Windows through test normality, homogenity, and T test. Through the normality test obtained significance data > 0.05, homogeneity testing can be seen that from the pretest data from both obtained the value of probability value > &